CAS number：583-68-6
molecular formula：C7H8BrN
molecular weight：186.05
EINECS number：209-515-7

English synonyms

2-bromo-4-methyl-benzenamin;2-Bromo-4-methylbenzenamine;2-Bromo-4-toluidine;2-bromo-p-toluidin;2-Bromo-4-methylaniline,99%(4-Amino-3-bromtoluol);2-Bromo-p-toluid;4-Amino-3-bromotoluene~2-Bromo-p-toluidine;2-Bromo-4-methylanline

Related categories

Anilines; pharmaceutical intermediates; benzene series; halides; chemical linkage; intermediates; chemical raw materials; chemical intermediates; organic intermediates; AromaticHydrocarbons (substituted) & Derivatives; Amines; blocks; Bromides;

Introduction

colorless liquid. The melting point is 26°C, the boiling point is 240°C, the relative density is 1.500, and the refractive index is 1.6020. Miscible with alcohol and ether, insoluble in water. Organic synthesis intermediates.

colorless liquid. The melting point is 26°C, the boiling point is 240°C, the relative density is 1.500, and the refractive index is 1.6020. Miscible with alcohol and ether, insoluble in water.

●  Organic Synthesis Intermediates

●  Heating p-toluidine and glacial acetic acid under reflux for 2 hours is converted into N-acetyl p-toluidine, cooled to 45°C, and bromine is added dropwise, and the bromination reaction is controlled at 50-55°C. The reactant was injected into an aqueous solution of sodium sulfite, and 3-bromo-4-acetamidotoluene was precipitated. Then it is hydrolyzed with concentrated hydrochloric acid, and the resulting hydrochloride reacts with sodium hydroxide solution to obtain free 2-bromo-4-methylaniline. Yield 51-57%.